665-674_GCappforensic.qxp
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GC CHROMATOGRAMS | CLINICAL, FORENSIC & TOXICOLOGY
Solvents, Cocaine Solvents Rtx®-BAC1 & Rtx®-BAC2 (headspace analysis) Rtx®-BAC1, 30m, 0.53mm ID, 3.0μm (cat.# 18001)
Rtx®-BAC2, 30m, 0.53mm ID, 2.0μm (cat.# 18000) 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17.
GC_PH00509
ethyl chloride diethyl ether methylene chloride acetonitrile methyl tert-butyl ether chloroform methyl ethyl ketone 1,1,1-trichloroethane benzene trichloroethylene toluene 1,1,2-trichloroethane tetrachloroethene p-xylene m-xylene o-xylene tetrachloroethane
GC_PH00510
Sample: Oven temp.: Inj./det. temp.: Carrier gas: Linear velocity: Det.:
1.0mL headspace sample 40°C (hold 5 min.) to 240°C @ 5°C/min. 240°C helium 65cm/sec. FID
Cocaine & Cocaine Adulterants Rtx®-440
1. 2. 3. 4. 5. 6. 7. 8.
benzocaine phenacetin prilocaine lidocaine caffeine procaine cocaine tetracaine
Chromatogram Search Tool Search by compound name, synonym, CAS # or keyword
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GC_PH00770
Column: Sample: Inj.: Inj. temp.: Carrier gas: Flow rate: Oven temp.: Det.: Transfer line temp.: Scan range: Ionization: Mode:
Rtx®-440, 30m, 0.25mm ID, 0.50µm (cat.# 12938) 100µg/mL each compound in methanol 1.0µL split (split ratio 1:10), laminar cup splitter inlet liner (cat.# 20801) 250°C helium, constant flow 1mL/min. 150°C to 275°C @ 25°C/min., to 300°C @ 15°C/min. (hold 5.0 min.) MS 180°C 35-550amu EI scan
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Mar 2011
