698-703_GCappChem.qxp
11/19/2008
5:13 PM
Page 699
GC APPLICATIONS | SOLVENTS & CHEMICALS
Solvents, Ketones, Amines Solvents Rt®-QS-BOND
NEW!
1. 2. 3. 4. 5. 6. 7. 8. 9.
Ketones Rt®-QS-BOND
methanol acetonitrile methylene chloride trans-1,2-dichloroethylene cis-1,2-dichloroethylene tetrahydrofuran 1,4-dioxane toluene ethylbenzene
1. 2. 3. 4.
Inj. temp.: Carrier gas: Flow rate: Oven temp.: Det.:
acetone 2-butanone 2-hexanone 4-methyl-2-pentanone
GC_PC01015
GC_PC01021
Column: Sample: Inj.:
NEW!
Rt®-QS-BOND, 30m, 0.53mm ID (cat.# 19738) 100-1,000µg/mL solvent mix in DMSO:water, 60:40 (v/v) 1µL split (split ratio 5:1), 4mm Siltek® single gooseneck liner (cat.# 20798-214.1) 240°C helium, constant flow 5.7mL/min. @ 40°C 40°C (hold 0.5min.) to 120°C @ 15°C/min. to 200°C @ 5°C/min. (hold 10 min.) FID @ 240°C
Column: Sample: Inj.: Inj. temp.: Carrier gas: Flow rate: Oven temp.: Det.:
Rt®-QS-BOND, 30m, 0.53mm ID (cat.# 19738) 1,000µg/mL VOA Calibration Mix #1 (ketones) (cat.# 30006) in methanol:water, 90:10 (v/v) 1µL split (split ratio 50:1), 4mm Siltek® single gooseneck liner (cat.# 20798-214.1) 240°C helium, constant flow 5.7mL/min. @ 40°C 60°C to 225°C @ 15°C/min. (hold 10 min.) FID @ 240°C
Ethanolamines Rtx®-35 Amine
Ethanolamines Rtx®-5 Amine 1 3
1. monoethanolamine 2. diethanolamine 3. triethylene glycol monomethylether (IS) 4. triethanolamine
2 4
GC_CH00585
1. 2. 3. 4. min.
5
10 GC_CH00296
Column: Sample: On-column conc.: Oven temp.: Inj./det. temp.: Carrier gas: Linear velocity: FID sensitivity: Split ratio:
monoethanolamine diethanolamine triethyleneglycol monomethylether triethanolamine
Rtx®-5 Amine, 15m, 0.25mm ID, 0.50µm (cat.# 12335) 1.0µL split injection of ethanolamine mix in methanol 34ng 50°C (hold 2 min.) to 180°C @ 10°C/min. (hold 2 min.) 280°C/300°C hydrogen 43cm/sec. set @ 50°C 6.4 x 10-11 AFS 58:1
800-356-1688 or 814-353-1300
Column: Sample: Inj.: Inj. temp.: Carrier gas: Linear velocity: Oven temp.: Det.:
Rtx®-35 Amine, 30m, 0.32mm ID, 1.0µm (cat.# 11354) 500µg/mL ethanolamine standard in water 1.0µL split (split ratio 10:1), cup splitter inlet liner (cat.# 20709) 300°C helium, constant pressure 40cm/sec. @ 50°C 50°C (hold 0.50 min.) to 280°C @15°C/min. FID @ 300°C
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