720
Antiepileptics Antiepileptics (Underivatized) Rtx®-20 1
G C A P P L I C AT I O N S | P H A R MAC E U T I C A L
11
2
Column: Sample: Conc.: Oven temp.:
6 3
4 10 7
8 9
12
5
min.
5
10
15
Inj./det. temp.: Det.: Carrier gas: Linear velocity: FID sensitivity: Split ratio:
20
GC_PH00265
Antiepileptics (Underivatized) Rtx®-1701
Rtx®-20, 15m, 0.32mm ID, 0.50µm (cat.# 10336) 1.0µL split injection of antiepileptic drugs 1000ng/µL 150°C to 280°C @ 7°C/min. (hold 5 min.) 250°C/270°C FID helium 30cm/sec. set @ 150°C 1.28 x 10-10 AFS 30:1
1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12.
valproic acid ethosuximide methsuximide phensuximide desmethyl methsuximide mephenytoin ethotoin PEMA phenobarbital primidone carbamazepine diphenylhydantoin
1 11
Column:
3
Sample: Conc.: Oven temp.:
6
2
Inj./det. temp.: Det.: Carrier gas: Linear velocity: FID sensitivity: Split ratio:
4 7
8 9 10
5 12
min.
5
10
15 GC_PH00266
Phone: 800-356-1688 or 814-353-1300 www.restek.com
20
Rtx®-1701, 15m, 0.32mm ID, 0.50µm (cat.# 12036) 1.0µL split injection of antiepileptic drugs 1000ng/µL 150°C to 280°C @ 7°C/min. (hold 5 min.) 250°C/270°C FID helium 30cm/sec. set @ 150°C 1.28 x 10-10 AFS 30:1
