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672 Food Contaminants Organochlorine and Organophosphorus Pesticides FAPAS® Proficiency Testing Rxi®-5ms G C A P P L I...

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Food Contaminants Organochlorine and Organophosphorus Pesticides FAPAS® Proficiency Testing Rxi®-5ms

G C A P P L I C AT I O N S | F O O D S , F L AV O R S , & F R AG R A N C E S

Rxi® Technology!

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15.

dichlorvos methacrifos α-BHC hexachlorobenzene δ-BHC (lindane) β-BHC diazinon etrimphos phosphamidon chlorpyrifos-methyl heptachlor fenitrothion pirimiphos methyl malathion aldrin

Column: Sample:

Inj.: Instrument: Inj. temp.: Carrier gas: Flow rate: Oven temp.:

GC_FF00826

Organochlorine and Organophosphorus Pesticides FAPAS® Proficiency Testing Rxi®-5ms

Rxi® Technology!

Det.: Transfer line temp.: Scan range: Solvent delay: Tune: Ionization:

1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17.

Sample:

Inj.:

Instrument: Inj. temp.: Carrier gas: Flow rate: Oven temp.: GC_FF00827

Det.: Transfer line temp.: Scan range: Solvent delay: Tune: Ionization:

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chlorpyrifos heptachlor epoxide oxychlordane trans-chlordane endosulfan I cis-chlordane 2,4'-DDT dieldrin endrin endosulfan II 4,4'-DDE 4,4'-DDD endosulfan sulfate 4,4'-DDT

Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423) FAPAS® Series 5 OC Pesticide Mix 1 (cat.# 32412), FAPAS® Series 9 OP Pesticide Mix 1 (cat.# 32413) 1.0µL, 10ppm each analyte, split (10:1) 4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771) Agilent 6890 290°C helium, constant flow 1.2mL/min. 100°C (hold 0.5 min.) to 300°C @ 7°C/min. (hold 1 min.) Agilent 5973 GC/MS 280°C 35-550amu 4 min. DFTPP EI

naphthalene-d8 dichlorvos acenaphthene-d10 methacrifos α-BHC hexachlorobenzene δ-BHC (lindane) β-BHC phenanthrene-d10 diazinon etrimphos phosphamidon chlorpyrifos-methyl heptachlor fenitrothion pirimiphos methyl malathion

Column:

16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29.

18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34.

aldrin chlorpyrifos heptachlor epoxide oxychlordane trans-chlordane endosulfan I cis-chlordane 2,4'-DDT dieldrin endrin endosulfan II 4,4'-DDE 4,4'-DDD endosulfan sulfate 4,4'-DDT chrysene-d12 perylene-d12

Rxi®-5ms, 30m, 0.25mm ID, 0.25µm (cat.# 13423) FAPAS® Series 5 OC Pesticide Mix 1 (cat.# 32412), FAPAS® Series 9 OP Pesticide Mix 1 (cat.# 32413), SV Internal Standard Mix (cat.# 31206) 1.0µL, 10ppm each analyte, split (10:1) 4mm Drilled Uniliner® inlet liner (hole near bottom) (cat.# 20771) Agilent 6890 290°C helium, constant flow 1.2mL/min. 100°C (hold 0.5 min.) to 300°C @ 7°C/min. (hold 1 min.) Agilent 5973 GC/MS 280°C 35-550amu 4 min. DFTPP EI