Essential Oils Lemon Oil Rtx®-5 7,8 2 35
15 6
14 38 29
32 33
36 17 26 13 35
12
9
4
10 11
20
21 22
19 18
24 23
16
27,28
25
37
31 34
30
1 min.
2
4
6
8
10
12
Column: Sample: Oven temp.: Inj./det. temp.: Carrier gas: Linear velocity: FID sensitivity: Split ratio:
14 16 GC_FF00138
18
20
22
24
26
28
Rtx®-5, 30m, 0.32mm ID, 0.25µm (cat.# 10224) Wet needle split injection of a neat lemon oil 75°C (hold 8 min.) to 250°C @ 4°C/min. 250°C hydrogen 40cm/sec. (flow rate: 3.2cc/min.) 2 x 10-11 AFS 100:1
heptanol α-thujene α-pinene camphene sabinene β-pinene 6-methyl-5-hepten-2-one myrcene octanal α-phellandrene 3-carene α-terpinene p-cymene limonene γ-terpinene octanol terpinolene linalool nonanal citronellal terpinene-4-ol α-terpineol decanol octyl acetate nerol neral carvone geraniol geranial nonyl acetate citronellyl acetate neryl acetate geranyl acetate dodecanal β-caryophyllene trans-α-bergamotene α-humulene β-bisabolene
Spearmint Oil (Native ) Stabilwax®
1
2
13
4 6 7
25
19
15
16
3
18 28
21
17
29 24
8
5
min.
4
6
30
12
9 10
20 22
11
8
23
14 10
12
26 27
14
16
18
20
22
24
26
28
30
32
GC_FF00140
Column: Sample: Oven temp.: Inj./det. temp.: Carrier gas: Linear velocity: FID sensitivity: Split ratio:
Stabilwax®, 60m, 0.25mm ID, 0.25µm (cat.# 10626) 0.2µL split injection of a neat spearmint oil 75°C (hold 4 min.) to 200°C @ 4°C/min. (hold 10 min.) 250°C hydrogen 40cm/sec. set @ 160°C 4 x 10-11 AFS 100:1
1. 2. 3. 4. 5. 6. 7. 8. 9. 10.
α-pinene β-pinene sabinene myrcene α-terpinene l-limonene 1,8-cineole cis-ocimene γ-terpinene p-cymene
11. 12. 13. 14. 15. 16. 17. 18. 19. 20.
terpinolene 3-octyl acetate 3-octanol l-menthone trans-sabinenehydrate β-bourbonene linalool terpinene-4-ol β-caryophyllene dihydrocarvone
21. 22. 23. 24. 25. 26. 27. 28. 29. 30.
trans-dihydrocarvyl acetate β-farnesene α-terpineol germacrene-∆ carvone cis-carvyl acetate trans-carveol cis-carveol cis-jasmone viridiflorol
Phone: 800-356-1688 or 814-353-1300 www.restek.com
G C A P P L I C AT I O N S | F O O D S , F L AV O R S , & F R AG R A N C E S
1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. 29. 30. 31. 32. 33. 34. 35. 36. 37. 38.
659
