552
SSRIs, Anti-Diabetic, Anti-Ulcerative Selective Serotonin Reuptake Inhibitors (SSRIs) on pHidelity® C18, pH 11 Peak List 1. uracil (marker) 2. fluvoxamine maleate 3. fluoxetine 4. sertraline HCl
H P LC A P P L I C AT I O N S | P H A R MAC E U T I C A L
Sample: Inj.: 10µL Conc.: 100µg/mL each component Sample diluent: acetonitrile Column: Cat.#: Dimensions: Particle size: Pore size:
pHidelity® C18 9579365 150mm x 4.6mm 3µm 200Å
Conditions: Mobile phase: Flow: Temp.: Det.:
10mM ammonium bicarbonate (pH 11): acetonitrile:tetrahydrofuran, 45:45:10 1.5mL/min. ambient UV @ 230nm
LC_PH0361
Anti-Diabetic Glyburide (Glybenclamide) on Ultra IBD
Anti-Ulcerative Cimetidine on Ultra IBD (LC/MS)
2
Peak List: 1. cimetidine Peak List: 1. unknown 2. glyburide Sample: Inj.: Conc.: Solvent:
Sample: Inj.: Conc.: Solvent:
Column: Cat.#: Dimensions: Particle size: Pore size:
5µL 10µg/mL mobile phase
Conditions: Mobile phase:
1µL 500mg/mL water:methanol:acetone (1:1:2, v/v)
Column: Cat.#: Dimensions: Particle size: Pore size: Conditions: Mobile phase: Flow rate: Temp.: Det.:
Ultra IBD 9175552 50mm x 2.1mm 5µm 100Å
Ultra IBD 9175565 150mm x 4.6mm 5µm 100Å
1
Flow: Column temp.: Det.: Interface: Ion mode: Ion spray voltage: Temp.: Orifice: Ring: Auxiliary gas:
water:acetonitrile (20:80, v/v) 0.2mL/min. ambient PE/Sciex API 150 EX turbo ion spray positive 4800V 350°C 10V 100V 6000cc/min.
water with 0.1% (v/v) acetic acid: acetonitrile (95:05, v/v) 1.0mL/min. 27°C UV @ 254nm
1
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1
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min.
LC_0069
Phone: 800-356-1688 or 814-353-1300 www.restek.com
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1.0 LC_0115
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